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العنوان
Preparation and Characterization of Cellulosic Bionanocomposites Using Local Agriculture Residues /
المؤلف
Seleim, Wafaa Seleim AvouEl-Seoud.
هيئة الاعداد
باحث / وفاء سليم أبو السعود سليم
مشرف / أحمد مؤمن محمد منير المصرى
مشرف / محمد لطفى حسن
مشرف / صفاء خليل حسن
الموضوع
Characters and characteristics. Agriculture - Réunion - Congresses.
تاريخ النشر
2013.
عدد الصفحات
134 p. :
اللغة
الإنجليزية
الدرجة
ماجستير
التخصص
الكيمياء الحيوية ، علم الوراثة والبيولوجيا الجزيئية
تاريخ الإجازة
1/1/2013
مكان الإجازة
جامعة الزقازيق - كلية العلوم - كيمياء
الفهرس
Only 14 pages are availabe for public view

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Abstract

Cellulose nanocrystals (CNC) isolated from bagasse, rice straw and palm rachis by hydrolysis using sulfuric acid 65% (wt/wt) with length 76-101 nm for bagasse, 75-104 nm for rice straw and 209-416 nm for palm rachis. Cellulose nanocrystals suspension used with polymers like alginate, chitosan, gelatin and PVA for synthesizing polymer/CNC nanocomposites by casting method at different concentrations of CNC [from 2.5-20% (wt/wt)]. Cellulose nanocrystals were characterized by Transmission Electron Microscopy (TEM), X-ray Diffraction (XRD) and Fourier transform infra red (FTIR). Nanocompsites films were characterized by Scanning Electron Microscope (SEM), X-ray Diffraction (XRD), Dynamic Mechanical Thermal Analysis (DMTA), tensile strength and moisture sorption properties. Rheological properties of polymer/ CNC mixture were also studied. Biodegradation of the nanocomposites films in Tris(hydroxymethyl)aminomethane solution was studied.