Search In this Thesis
   Search In this Thesis  
العنوان
Study in The Use of Some Advanced Separation Techniques /
المؤلف
Abd-Allah, Ibrahim Ahmed Said.
هيئة الاعداد
باحث / إبراهيم أحمد سعيد عبد الله
مشرف / يحيى عبد القادر الطويل
مشرف / محمد حلمى عبد العزيز
مناقش / أحمد أمين عبد العظيم زعطوط
مناقش / منى السيد عثمان
الموضوع
Chemical Reactors.
تاريخ النشر
2013.
عدد الصفحات
84 p. :
اللغة
الإنجليزية
الدرجة
ماجستير
التخصص
الهندسة (متفرقات)
تاريخ الإجازة
1/8/2013
مكان الإجازة
جامعة الاسكندريه - كلية الهندسة - هندسة كيميائية
الفهرس
Only 14 pages are availabe for public view

from 124

from 124

Abstract

The aim of the present work is to develop a multi rotating disc electrochemical reactor and catalytic reactor of high space time yield suitable for conducting catalytic and electrochemicalliquid-solid diffusion controlled reactions.
The performance of multi rotating disc electrochemical reactor in removing copper IOns from a synthetic waste water solution was examined under different operating conditions.
Before testing the performance of the multi rotating disc electrochemical reactor in copper deposition, the effect of surface roughness on the rate of mass transfer was first studied using a single rough rotating disc by measuring the limiting current of the cathodic reduction of K3Fe(CN)6 in a large excess ofNaOH.
Variables studied were:
1- Disc rotation speed.
2- Degree of surface roughness.
3- Distance between rotating discs within the multi disc cathode.
4- Physical properties of the solution (p, J.l and D).
The present study revealed the following results:
1. The mass transfer coefficient was found to increase with disc rotation speed.
2. The mass transfer coefficient was found to increase by increasing the degree of
roughness.
3. Mass transfer data were correlated using the method of dimensional analysis; for
the conditions 1253<Sc< 2778, 13584.7< Re < 108682 and
0.007142«e/d)<0.02857, the following overall mass transfer correlation was obtained:
Sh = 2.695 Scl/3 Reo 54 (e/d) 0.276
With an average deviation of ± 7.4%