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العنوان
Electrochemical synthesis of a modified graphite sensor based on nanoparticles /
الناشر
Mohammed Shehata Otiefy Ahmed ,
المؤلف
Mohammed Shehata Otiefy Ahmed
هيئة الاعداد
باحث / Mohammed Shehata Otiefy Ahmed
مشرف / Amany Mohamed Fekry
مناقش / Amany Mohamed Fekry
مناقش / Amany Mohamed Fekry
تاريخ النشر
2019
عدد الصفحات
128 P. :
اللغة
الإنجليزية
الدرجة
الدكتوراه
التخصص
Physical and Theoretical Chemistry
تاريخ الإجازة
15/12/2019
مكان الإجازة
جامعة القاهرة - كلية العلوم - (Physical Chemistry)
الفهرس
Only 14 pages are availabe for public view

from 220

from 220

Abstract

Novel promising electrochemical Caffeine (Caf) sensors were achieved through various ways. Firstly by chemical mixing of Co (II, III) Oxide Nanoparticles on a carbon paste electrode (CPE), secondly by chemical mixing of graphene oxide (GO) nanoparticles and reduced glutathione (GSH) with CP, thirdly by mixing multiwalled carbon nanotubes (MWCNT) and zeolite (Zeo) with CP and/or finally electrodeposition of Ag- nanoparticles on cellulose acetate phthalate (CAP) and chitosan (Chit) polymers with CP. Electrochemical techniques including cyclic voltammetry (CV), electrochemical impedance spectroscopy (EIS), chronoamperometry (CA) and differential pulse voltammetry (DPV) were used in the present investigation in addition to analysis techniques like Scanning Electron Microscope (SEM), Transmission Electron Microscope (TEM), Energy Dispersive X-Ray (EDX) and X-Ray Diffraction (XRD) techniques, in both aqueous and surfactant modified media using sodium dodecyl sulphate (SDS). Caf measurements were investigated in various supporting solutions of pH range (0.75-5.00) containing 0.5 mmol L-1 of SDS. Acceptable results were attained for the finding of Caf in real samples as beverages and drug samples