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Abstract I’he p resent thes i s comprises t he followi ng parts . An introducti on which ’ ”elate!; the diffe rent components o f t he wo r k to a c l ear aim . Tliis aim is to elabo rate a p roced uro for t he successivo deter. i nation of ga l lium . i nd ium and thllllium In II mixture of tho t.nree ana l yt..,s . The I iterature collection o f t he spec t r ometric de t e rmi nation of t he t hree ilnal yt es ind i ell tes thll t such procedures IIre , in gene ral. JrH..”OnIparably s uper i o r to all e he.ica l p rocedurea fo r the de t ect i on and dete rmination of the i ndividuill ana l yLe in iI VatHtL y of matri ces . Event ual l y. no compre hensive procedure has been elaborat ed t o determine 011 the three ana l ytes in a mixture wi thout using separat i on techni ques. In the saMe con t ext . severa l very s uccess fu l li t t empts have been .. ade Lo predict the cond i tions f or c arrying out an,.lytiClIi cOlllp i exoIII(!tric determinati o ns of the t hree a na .l ytes. Such attempts having s ho”l11 that the possibility of direct comp le xomet r ic titration i s de t ermined by the value o f the st,.bi I ity constant of t he corresponding compl ex . Lho i n itial co ncent rati o n of the r ea gents . t he pll •.. . etc. Howe-ver . on ly a comparat ive l y sIMll number o f papers dea l wilh the quantitative approach to the de t o rmi nation o f two of the three analytes. |