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العنوان
The physical properties of some polymeric composites /
المؤلف
El­-Eshmawi, Islam Shokry Ahmed.
هيئة الاعداد
باحث / إسلام شكري أحمد العشماوي
مشرف / حامد إبراهيم عبدالقادر
مناقش / نجوى عبدالحكيم محمد يوسف
مناقش / نجاح عبدالرحيم الششتاوي
الموضوع
BiCl3. LaNi3Co2. filled PVDF films. FTIR. XRD. SEM. DSC. DC electrical conductivity.
تاريخ النشر
2005.
عدد الصفحات
156 p. :
اللغة
الإنجليزية
الدرجة
الدكتوراه
التخصص
الفيزياء وعلم الفلك
تاريخ الإجازة
1/1/2005
مكان الإجازة
جامعة المنصورة - كلية العلوم - Lecturer ­ Physics
الفهرس
Only 14 pages are availabe for public view

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Abstract

The present work deals with spectroscopic, thermal, electrical and magnetic investigations of PVDF films filled/composites BiCl3, LaNi3Co2, SmNi3Co2, and TbNi3Co2. Spectroscopic and thermal investigations were carried out for the prepared films using Fourier Transform Infrared (FTIR), X­ray diffraction (XRD), Scanning Electronic Microscopy (SEM) and Differential Thermal Analysis (DTA) or Differential Scanning Calorimetry (DSC). Also, DC electrical resistivity ((Su? (Band Magnetoresistance (MR) were measured. The FTIR analysis detected the presence of ga­ sand gb­sphases and head­to­head and tail­to­tail polymer chain defects. The maximum and minimum value of h­to­h was fount at 35% and 60%, respectively. These results were confirmed by XRD and DSC analysis. X­ray analysis confirmed the presence of ga­ sand gb­sphase. In DSC therograms, a sharp endothermic peak at T1 <U+2248> 444 K was due to melting. This peak was used to calculate the order of reaction, which was n <U+2248> 1, indicating an undecompsed reactants, and the activation energy of melting. DC electrical conduction was attributed to the one dimensional interpolaron hopping mechanism.